In Kjeldahl’s method, which base is used to liberate ammonia from the digested sample?
NaOH is added to the digested sample ( (NH₄)2SO₄ ) to liberate NH₃, which is then distilled and titrated. This follows from NCERT principle where the relation explains the outcome clearly for students in simple steps.
Ref: NCERT Chemistry Textbook for Class XI and XII, Chapter: Some Basic Concepts, Structure of Atom and Periodicity, Topic: Mole concept, atomic models and periodic trends.